HCID 68530103, compound → HCID 68527303, compound

Participants

Reaction Steps

1.1 g (5.46 mmoles) of the product of Step 1 are dissolved in 30 mL of methanol (MeOH). 30 mL of (7N) ammoniacal methanol solution and 0.5 g of Raney nickel are added. The reaction mixture is hydrogenated overnight under a pressure of 1 bar, at ambient temperature. The catalyst is then filtered off and the filtrate is evaporated to dryness. The expected product is obtained in the form of an oil.

Provenance & Evidence