HCID 68974196, compound → HCID 68528606, compound

HRID 657570Notes

Reaction equation

HRID 657570 reaction equation
[CH2:1]1[CH:5]2[CH2:6][CH2:7][CH2:8][CH:4]2[CH2:3][N:2]1[C:9]([O:11][C:12]1[CH:13]=[C:14]2[C:17](=[CH:18][CH:19]=1)[CH:16]([CH2:20][N:21](C(OC(C)(C)C)=O)[CH2:22][CH2:23][C:24]([N:26]1[CH2:32][CH2:31][C:30]3[CH:33]=[C:34]([O:39][CH3:40])[C:35]([O:37][CH3:38])=[CH:36][C:29]=3[CH2:28][CH2:27]1)=[O:25])[CH2:15]2)=[O:10]>C(O)C.Cl>[CH2:1]1[CH:5]2[CH2:6][CH2:7][CH2:8][CH:4]2[CH2:3][N:2]1[C:9]([O:11][C:12]1[CH:13]=[C:14]2[C:17](=[CH:18][CH:19]=1)[CH:16]([CH2:20][NH:21][CH2:22][CH2:23][C:24]([N:26]1[CH2:32][CH2:31][C:30]3[CH:33]=[C:34]([O:39][CH3:40])[C:35]([O:37][CH3:38])=[CH:36][C:29]=3[CH2:28][CH2:27]1)=[O:25])[CH2:15]2)=[O:10]

Participants

4

Reactant 1

HCID 68974196HCID 68974196, compound

Product 1

HCID 68528606HCID 68528606, compound

Reagents, catalysts & solvents 2

HCID 313Hydrochloric AcidSolventHCID 702EthanolSolvent

Procedure

The product obtained in Step 1 is dissolved in 10 volumes of ethanol and 10 volumes of 3N ethanolic HCl solution. Stirring is carried out at ambient temperature for 24 hours and the precipitate obtained, which corresponds to the expected product, is filtered off.

Workup

  1. customthe precipitate obtained

Sources & evidence

ORD record
ord-ea1785e64e6945eba6708b69799f3668
Source dataset
uspto-grants-2011_12
Patent number
US08076325B2

Reaction notes

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