HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68971896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 68975923 | HCID 68975923 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68971896 | HCID 68971896 | — |
Reaction Steps
At ambient temperature, 2.63 g (4.5 mmol) of the compound obtained in Step B above are mixed into 120 mL of ethanol together with 25 mL of 3.7N ethanolic HCl. After stirring for 1 day at ambient temperature, the solid formed is filtered off, rinsed with ethanol and with ether and dried in vacuo to obtain the desired compound in the form of the hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076325B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-982fd8e1943e4a67a031f63e08e64fcc |
| Source note | uspto-grants-2011_12 |