Hydrochloric Acid → HCID 68971896, compound

HRID 657574Notes

Reaction equation

HRID 657574 reaction equation
C(OC(=O)[N:7]([CH2:23][CH2:24][C:25]([N:27]1[CH2:33][CH2:32][C:31]2[CH:34]=[C:35]([O:40][CH3:41])[C:36]([O:38][CH3:39])=[CH:37][C:30]=2[CH2:29][CH2:28]1)=[O:26])[CH2:8][CH:9]1[CH2:16][C:15]2[C:10]1=[CH:11][CH:12]=[C:13]([O:17][CH2:18][C:19]([NH:21][CH3:22])=[O:20])[CH:14]=2)(C)(C)C.[ClH:43]>C(O)C>[ClH:43].[CH3:39][O:38][C:36]1[C:35]([O:40][CH3:41])=[CH:34][C:31]2[CH2:32][CH2:33][N:27]([C:25](=[O:26])[CH2:24][CH2:23][NH:7][CH2:8][CH:9]3[CH2:16][C:15]4[C:10]3=[CH:11][CH:12]=[C:13]([O:17][CH2:18][C:19]([NH:21][CH3:22])=[O:20])[CH:14]=4)[CH2:28][CH2:29][C:30]=2[CH:37]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 68975923HCID 68975923, compound

Product 1

HCID 68971896HCID 68971896, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

At ambient temperature, 2.63 g (4.5 mmol) of the compound obtained in Step B above are mixed into 120 mL of ethanol together with 25 mL of 3.7N ethanolic HCl. After stirring for 1 day at ambient temperature, the solid formed is filtered off, rinsed with ethanol and with ether and dried in vacuo to obtain the desired compound in the form of the hydrochloride.

Workup

  1. customthe solid formed
  2. filtrationis filtered off
  3. washrinsed with ethanol and with ether
  4. customdried in vacuo

Sources & evidence

ORD record
ord-982fd8e1943e4a67a031f63e08e64fcc
Source dataset
uspto-grants-2011_12
Patent number
US08076325B2

Reaction notes

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