HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 68905693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 68909667 | HCID 68909667 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68905693 | HCID 68905693 | 2.6% |
Reaction Steps
A Following the procedure of example 42§A, but starting from 1-(3-{[4′-(2-piperidinocarbonylethen-1-yl)biphenyl-4-yl]oxy}propyl)piperidine (0.6 g) and lithium aluminum hydride (120 mg) in tetrahydrofuran (15 mL) affords 15 mg of 1-(3-{[4′-(3-piperidinoprop-1-en-1-yl)biphenyl-4-yl]oxy}propyl)piperidine as pale yellow crystals melting at 100-105° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076329B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-1683ef31f7944ae590d0745dfa350512 |
| Source note | uspto-grants-2011_12 |