HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 23150278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (Pyridin-4-yl)boronic acid | HCID 2734379 | — |
| Reactant | 1-Bromo-4-(3-chloropropoxy)benzene | HCID 12685609 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23150278 | HCID 23150278 | 85% |
Reaction Steps
Following the procedure described in example 24, but starting from 1-bromo-4-(3-chloropropoxy)benzene (2.5 g), potassium carbonate (4.14 g), 4-pyridylboronic acid (1.47 g) and palladium tetrakistriphenylphosphine (116 mg) in toluene (24 mL) affords 2.11 g of 4-[4-(3-chloropropoxy)phenyl]pyridine as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076329B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-51cc0671333b42e6ba8e134aff4632ae |
| Source note | uspto-grants-2011_12 |