HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glutaric Acid → HCID 178484388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glutaric Acid | HCID 743 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 178484382 | HCID 178484382 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178484388 | HCID 178484388 | 65.9% |
Reaction Steps
10.0 g of the metformin free-base and 3.98 g of glutaric acid were stirred in 100 ml of methyl alcohol at a temperature of 40° C., and then ethyl acetate was added thereto. The produced crystal was filtered and dried in hot air, thus obtaining 5.15 g (yield: 43.8%) of metformin glutarate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076377B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-d99303c04d69446cad2b4281e2f52d51 |
| Source note | uspto-grants-2011_12 |