HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Chloro-3-nitrophenyl)methanol → 2-Chloro-3-nitrobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Chloro-3-nitrophenyl)methanol | HCID 15132843 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Chloro-3-nitrobenzaldehyde | HCID 12667713 | — |
Reaction Steps
9.2 g (49.05 mmol) of (2-chloro-3-nitrophenyl)methanol and 13.2 g (151.8 mmol) of activated manganese(IV) oxide in 50 ml of chloroform are heated under reflux for 20 h. The mixture is filtered through kieselguhr, concentrated and dried under high vacuum. The resulting title compound is directly reacted further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076355B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-396e3c02c73c40b7b6210436ec567935 |
| Source note | uspto-grants-2011_12 |