HCID 66744672, compound → HCID 66743967, compound

Participants

Reaction Steps

(R)-1-(5-tert-Butoxy-2-isopropoxy-benzothiazol-7-yl)-2-(1,1-dimethyl-2-phenyl-ethylamino)-ethanol (40 mg) is stirred in formic acid (2 ml) for 72 hours. The formic acid is removed in vacuo and the title compound is obtained by reversed phase column chromatography using a Jones Flashmaster Personal™ flash chromatography system (ISOLUTE FLASH C18, gradient elution AcCN/water 0 to 50%). MS (ES+) m/e 359.26 (MH+) LCT57144

Provenance & Evidence