HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-6-nitrobenzoxazole → 2-Methyl-1,3-benzoxazol-6-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-6-nitrobenzoxazole | HCID 79766 | — |
| Reactant | Thiophene, 1,1-dioxide | HCID 117926 | — |
| Product | 2-Methyl-1,3-benzoxazol-6-amine | HCID 590539 | — |
Reaction Steps
This compound was prepared from 2-methyl-6-nitrobenzoxazole (2.0 g, 13.5 mmol) in the same manner described for 5-aminobenxo[b[thiophene 1,1-dioxide, affording 1.57 (94%) of the title compound as a brown solid. MS LC-MS (M+H)+=149.1, RT=0.77 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076488B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-acc7a31ccb0249e498547c6fc92de01a |
| Source note | uspto-grants-2011_12 |