HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-amino-N-methylacetamide hydrochloride → HCID 58385419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-amino-N-methylacetamide hydrochloride | HCID 13842202 | — |
| Reactant | 4-(4-Aminophenoxy)pyridine-2-carboxylic acid methylcarbamoylmethylamide | HCID 68429577 | — |
| Product | HCID 58385419 | HCID 58385419 | — |
Reaction Steps
The title compound was prepared in the same manner described for 4-(4-aminophenoxy)pyridine-2-carboxylic acid methylcarbamoylmethylamide, substituting 2-amino-N,N′-dimethylacetamide hydrochloride for 2-amino-N-methylacetamide hydrochloride. 1H-NMR (DMSO-d6) δ 8.75 (t, J=4.8 Hz, 1H), 8.49 (d, J=5.4 Hz, 1H), 7.33 (d, J=2.7 Hz, 1H), 7.32 (d, J=2.7 Hz, 1H), 6.86 (d, J=8.7 Hz, 2H), 6.63 (d, J=9.0 Hz, 2H), 5.18 (s, 2H), 4.11 (d, J=5.4 Hz, 2H), 2.96 (s, 3H), 2.85 (s, 3H); MS LC-MS [M+H]+=315.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076488B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-b67ebb49ea4f45389e0d4a8751588112 |
| Source note | uspto-grants-2011_12 |