N-(2-Aminoethyl)piperidine → HCID 59987498, compound

Participants

Reaction Steps

The title compound was prepared in the same manner described for 4-[3-({[(1-methyl-1H-indazol-5-yl)amino]carbonyl}-amino)phenoxy]-N-(2-piperidin-1-ylethyl)pyridine-2-carbox-amide, substituting 3-aminopyridine for 1-(2-aminoethyl)piperidine. 1H-NMR (DMSO-d6) δ 10.39 (s, 1H), 8.93 (s, 1H), 8.72 (s, 1H), 8.63 (d, J=5.4 Hz, 1H), 8.38 to 8.36 (m, 1H), 8.19 (d, J=8.4 Hz, 1H), 7.91 to 7.86 (m, 3H), 7.85 to 7.51 (m, 3H), 7.42 (t, J=2.1 Hz, 1H), 7.52 to 7.17 (m, 4H), 6.85 (dd, J=2.4, 1.5 Hz, 1H), 3.98 (s, 3H); MS LC-MS (M+H)+=480.1, RT=2.81 min.

Provenance & Evidence