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HRID65853

反应详情

EQUATION

反应方程式

HRID 65853 的结构方程式

REACTANTS

反应物

3
结构：NNc1ccccc1
HCID7516

Phenylhydrazine

C6H8N2

结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：COc1ccccc1S(=O)(=O)OCC(=O)c1ccccc1
HCID86736197

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccccc1S(=O)(=O)OCC(=NNc1ccccc1)c1ccccc1
HCID86736196

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

Into a reactor, equipped with a Dean-Stark separator, were introduced 100 ml of benzene, 1 ml of acetic anhydride, 10.8g (0.1 mol) of phenylhydrazine and 30.6 g (0.1 mol) of 3-methoxy-4-benzenesulphonyloxy-acetophenone. The reaction medium was stired and refluxed for 1 hour.

WORKUP

后处理

  1. customInto a reactor, equipped with a Dean-Stark separator
  2. temperaturerefluxed for 1 hour