HRID6587

反应详情

EQUATION

反应方程式

HRID 6587 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2.2 g of [R]-1-trifluoromethylheptyl 4-benzyloxybenzoate, (13) 100 mg of PdOH/C in 50 ml of ethyl acetate was stirred at RT over night under H2 atmosphere. Then the catalyst was filtered out and filtrate was evaporated to dryness to give the pure compound in yield of 99%.

WORKUP

后处理

  1. filtrationThen the catalyst was filtered out
  2. customfiltrate was evaporated to dryness
  3. customto give the pure compound in yield of 99%