HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-((2-Fluorophenyl)methoxy)benzaldehyde → 3,4,5-Trimethoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-((2-Fluorophenyl)methoxy)benzaldehyde | HCID 702717 | — |
| Reactant | 4-[(3-Fluorophenyl)methoxy]-3-[(3-fluorophenyl)methyl]benzaldehyde | HCID 86631574 | — |
| Reactant | 3-(2-Fluorobenzyl)-4-(2-fluorobenzyloxy)benzaldehyde | HCID 86649329 | — |
| Solvent | 4-[(3-Fluorophenyl)methoxy]benzaldehyde | HCID 880119 | — |
| Product | 3,4,5-Trimethoxybenzaldehyde | HCID 6858 | — |
Reaction Steps
Calculate the percent content of 3-(2-fluorobenzyl)-4-(2-fluorobenzyloxy)benzaldehyde in the 4-(2-fluorobenzyloxy)benzaldehyde examined or of the 3-(3-fluorobenzyl)-4-(3-fluorobenzyloxy)benzaldehyde in the 4-(3-fluorobenzyloxy)benzaldehyde examined by internal standard calculation. The value of the limit of quantitation (LOQ) for (3-(2-fluorobenzyl)-4-(2-fluorobenzyloxy)benzaldehyde and of 3-(3-fluorobenzyl)-4-(3-fluorobenzyloxy)benzaldehyde is 0.005% by weight. The value of the limit of detection (LOD) for both considered impurities is 0.0025% by weight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076515B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-ba50b8b132004859921261c756d6a36f |
| Source note | uspto-grants-2011_12 |