Potassium Carbonate → HCID 59549299, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 5-chloro-2-hydroxy-benzaldehyde (7 g, 45 mmol), 2-bromo-2-methyl-propionic acid ethyl ester (10.4 g, 58 mmol), K2CO3 (18.6 g, 135 mmol) and KI (0.97 g, 5.8 mmol) in DMF (20 mL) was heated at 110° C. for 3 h. Then the mixture was filtered and the filtrate was concentrated. The residue was used into next step reaction without further purification (7 g).

Provenance & Evidence