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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 658972Generated: October 30, 2026

Trifluoroacetic acid → HCID 68777582, compound

https://huagongshe.com/reaction/658972

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 59585185HCID 59585185—
SolventDichloromethaneHCID 6344—
ProductHCID 68777582HCID 68777582—

Reaction Steps

To a stirred solution of tert-butyl 4-(3-methyl-2-oxo-2,3-dihydro-1H-imidazo[4,5-b]pyridin-1-yl)piperidine-1-carboxylate from Step B (73 mg, 0.22 mmol) in CH2Cl2 (5 mL) was added trifluoroacetic acid (2 mL). The resulting mixture was stirred at ambient temperature for 1 h then concentrated in vacuo to give the title compound. MS: m/z=233 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08080544B2
Source datasetuspto-grants-2011_12
ORD IDord-fcdcacac0a77404c9e8d0fdb85f202a1
Source noteuspto-grants-2011_12