HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68777582, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 59585185 | HCID 59585185 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68777582 | HCID 68777582 | — |
Reaction Steps
To a stirred solution of tert-butyl 4-(3-methyl-2-oxo-2,3-dihydro-1H-imidazo[4,5-b]pyridin-1-yl)piperidine-1-carboxylate from Step B (73 mg, 0.22 mmol) in CH2Cl2 (5 mL) was added trifluoroacetic acid (2 mL). The resulting mixture was stirred at ambient temperature for 1 h then concentrated in vacuo to give the title compound. MS: m/z=233 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08080544B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-fcdcacac0a77404c9e8d0fdb85f202a1 |
| Source note | uspto-grants-2011_12 |