HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 178464568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Ethanamine, 2,2,2-trifluoro- | HCID 9773 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Product | HCID 178464568 | HCID 178464568 | — |
Reaction Steps
TEA (1.3 mL, 0.8 mmol) was added to a solution of 2,2,2-trifluoroethylamine (72 mg, 1 mmol) and 1,1′-carbonyldiimidazole (135 mg, 0.8 mmol) in DMF (4 mL) (clear colorless solution). The solution was used for the synthesis of compound 5 without further isolation of compound 5a.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08080556B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-9b0ba0269e4b461aa12d78ae8c95a475 |
| Source note | uspto-grants-2011_12 |