HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 5-Ethyl-7-methyl-5H,7H-isoxazolo[3,4-d]pyrimidine-4,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 7-Methylisoxazolo[3,4-d]pyrimidine-4,6(5H,7H)-dione | HCID 12380620 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 5-Ethyl-7-methyl-5H,7H-isoxazolo[3,4-d]pyrimidine-4,6-dione | HCID 12380627 | — |
Reaction Steps
In 50 ml of dimethylformamide is dissolved 2 g of the 7-methyl-5H,7H-isoxazolo[3,4-d]pyrimidine-4,6-dione obtained in Example 19, followed by addition of 1.6 g of potassium carbonate and 2 ml of ethyl iodide. Then, the reaction and after-treatment are carried out in the same manner as Example 23 to obtain 0.9 g of the captioned compound as colorless crystals. melting point: 87°-88° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04129654 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-98d72dac1b174b2aa26bbefcff4156e1 |
| Source note | uspto-grants-1978_12 |