HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylthio-4,6-bis(trifluoromethyl)benzoic acid → N-((cis)-2-Cyclopentylamino-cyclopentyl)-2-methylsulfanyl-4,6-bis-trifluoromethyl-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylthio-4,6-bis(trifluoromethyl)benzoic acid | HCID 59347822 | — |
| Reactant | HCID 66681699 | HCID 66681699 | — |
| Product | N-((cis)-2-Cyclopentylamino-cyclopentyl)-2-methylsulfanyl-4,6-bis-trifluoromethyl-benzamide | HCID 51001237 | — |
Reaction Steps
The title compound, light pink solid, MS: m/e=455.3 [(M+H)+], was prepared in accordance with the general method of example 5 from (1RS,2SR)-N-Cyclopentyl-cyclopentane-1,2-diamine (intermediate AE) and 2-methylthio-4,6-bis(trifluoromethyl)benzoic acid (CAS 896120-49-3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08080541B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-44967390e2f642c18f5d07a59e3844c0 |
| Source note | uspto-grants-2011_12 |