HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 5-Chloro-2-methyl-6-nitro-1-indanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 5-Chloro-2-methyl-2,3-dihydro-1H-inden-1-one | HCID 21995614 | — |
| Product | 5-Chloro-2-methyl-6-nitro-1-indanone | HCID 22756382 | — |
Reaction Steps
According to Example 1 (a), 28.0 g (0.155 mole) of 5-chloro-2-methyl-1-indanone and 180 ml of fuming nitric acid yield the nitro compound having a melting point of from 75° to 78° C., which after recrystallization from ethanol rises to 87° to 89° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04129656 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-0faa3bdf0f024bf79037ff85cbe5db54 |
| Source note | uspto-grants-1978_12 |