HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 1,3-Dimethyl-3-(ethoxycarbonylperoxy)butyl ethyl carbonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 1,3-Dimethyl-3(ethoxycarbonylperoxy)butyl chloroformate | HCID 23346613 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1,3-Dimethyl-3-(ethoxycarbonylperoxy)butyl ethyl carbonate | HCID 23346605 | — |
Reaction Steps
To a solution of 24.4 g. (0.0786 mole) of (86.4%) 1,3-dimethyl-3(ethoxycarbonylperoxy)butyl chloroformate in 100 ml of diethyl ether, cooled at 10°±1° C was added a solution of 4.6 g (0.1 mole) of ethanol and 7.9 g. (0.1 mole) of pyridine in 25 ml of diethyl ether over a period of 20 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04129700 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-41234ce8fa264851a247626055a69791 |
| Source note | uspto-grants-1978_12 |