HuagongsheHuagongshe Chemistry Print Report · For research reference only
2',3'-Acetoxylidide → 4-[2-(2,3-Dimethyl-phenylamino)-oxazol-5-yl]-benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2',3'-Acetoxylidide | HCID 8656 | — |
| Reactant | 2-Acetylamino-4-aminotoluene | HCID 79492 | — |
| Reactant | 4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile | HCID 17757346 | — |
| Product | 4-[2-(2,3-Dimethyl-phenylamino)-oxazol-5-yl]-benzonitrile | HCID 24871997 | 91% |
Reaction Steps
The same procedure outlined above in the preparation of 4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile was used. However N-(2,3-dimethylphenyl)-acetamide was used instead N-(5-amino-2-methyl-phenyl)-acetamide. Yield=91%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08080669B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-17c3566efc694075a5cd1784ca2abf72 |
| Source note | uspto-grants-2011_12 |