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HRID65978

反应详情

EQUATION

反应方程式

HRID 65978 的结构方程式

REACTANTS

反应物

3
结构：c1ccncc1
HCID1049

Pyridine

C5H5N

结构：CCCCOC(=O)Cl
HCID61140

n-Butyl chloroformate

C5H9ClO2

结构：CC(CCO)CCCC(C)(C)OOC(C)(C)C
HCID53664183

未命名化合物

PRODUCTS

生成物

1
结构：CCCCOC(=O)OCCC(C)CCCC(C)(C)OOC(C)(C)C
HCID23346617

Butyl 7-(tert-butylperoxy)-3,7-dimethyloctyl carbonate

C19H38O5

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

2 次

PROCEDURE

实验过程

To a solution of 7.9 g (0.03 mole) of 3,7-dimethyl-7(t-butylperoxy)octyl alcohol and 2.4 g (0.03 mole) of pyridine in diethyl ether cooled at 10°±1° C was added a solution of 4.09 (0.03 mole) of n-butyl chloroformate in diethyl ether. The reaction temperature was maintained at 15°±1° C during the addition.

WORKUP

后处理

  1. temperatureThe reaction temperature was maintained at 15°±1° C during the addition