HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → Butyl 7-(tert-butylperoxy)-3,7-dimethyloctyl carbonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Butyl chloroformate | HCID 61140 | — |
| Reactant | 3,7-Dimethyl-7-(t-butylperoxy)octyl alcohol | HCID 53664183 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Butyl 7-(tert-butylperoxy)-3,7-dimethyloctyl carbonate | HCID 23346617 | — |
Reaction Steps
To a solution of 7.9 g (0.03 mole) of 3,7-dimethyl-7(t-butylperoxy)octyl alcohol and 2.4 g (0.03 mole) of pyridine in diethyl ether cooled at 10°±1° C was added a solution of 4.09 (0.03 mole) of n-butyl chloroformate in diethyl ether. The reaction temperature was maintained at 15°±1° C during the addition.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04129700 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-22cf3ce5ef674b899ba6e662b054e132 |
| Source note | uspto-grants-1978_12 |