Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Butyl disulfide → HCID 178454949, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Butyl disulfide | HCID 12386 | — |
| 반응물 | HCID 178503312 | HCID 178503312 | — |
| 반응물 | HCID 178506560 | HCID 178506560 | — |
| 용매 | Diethylether ethylacetate | HCID 21584169 | — |
| 생성물 | HCID 178454949 | HCID 178454949 | 18.4% |
반응 단계
Compound 21F was prepared following the procedure as described for the synthesis of compound 21A (see Scheme 3) using 1-butyldisulfanyl-butane as the disulfide and 3-(4-iodo-1H-pyrazol-3-yl)-pyridine (compound 20B). (flash chromatography conditions ethyl acetate/diethyl ether 3/1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08084473B2 |
| 출처 데이터셋 | uspto-grants-2011_12 |
| ORD ID | ord-5cd1dff7ccf94545a2b9e46a5563380d |
| 출처 메모 | uspto-grants-2011_12 |