HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorophenol → Methyl 5-chloro-2-[(2-fluorophenoxy)methyl]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorophenol | HCID 9707 | — |
| Reactant | Methyl 2-(bromoethyl)-5-chlorobenzoate | HCID 68983888 | — |
| Product | Methyl 5-chloro-2-[(2-fluorophenoxy)methyl]benzoate | HCID 68862280 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 1 from methyl 2-(bromoethyl)-5-chlorobenzoate and 2-fluorophenol: 1H-NMR (CDCl3) δ 8.02 (1H, d, J=2.4 Hz), 7.80-7.77 (1H, m), 7.57-7.53 (1H, m), 7.15-6.89 (4H, m), 5.52 (2H, s), 3.92 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084476B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-46c92a647ba7413584f6f972bd7951f7 |
| Source note | uspto-grants-2011_12 |