反应详情

A mixture of 2 (6.7 g, 1 mmol) in THF (100 ml) and EtOH (100 ml) is slowly added 10% Pd/C (680 mg) at room temperature. The reaction mixture is hydrogenated for 24 h with H2 balloon at room temperature. The mixture is filtered through celite pad and washed with EtOH. The filtrate is concentrated in vacuo.

1. customat room temperature
2. filtrationThe mixture is filtered through celite pad
3. washwashed with EtOH
4. concentrationThe filtrate is concentrated in vacuo