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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 660485Generated: October 29, 2026

Sodium Methoxide → HCID 68839456, compound

https://huagongshe.com/reaction/660485

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium MethoxideHCID 10942334—
ReactantHCID 68839807HCID 68839807—
SolventDichloromethane methanolHCID 21226129—
ProductHCID 68839456HCID 68839456—

Reaction Steps

To a stirred solution of 5-[2-benzyloxy-4-(1,2-dibromo-2-phenylethyl)-phenyl]-1,1-dioxo-1,2,5-thiadiazolidin-3-one (25 mg, 0.043 mmol) in MeOH/methylene chloride (1:1, 4 mL) is added NaOMe (0.17 mL, 0.086 mmol, 0.5M in THF). The solution is stirred at RT for 2 h and the solvent is removed under reduced pressure to give the title compound as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08084448B2
Source datasetuspto-grants-2011_12
ORD IDord-d69a816039ff44f4a2deb5d516db4bd6
Source noteuspto-grants-2011_12