HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 68839456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 68839807 | HCID 68839807 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 68839456 | HCID 68839456 | — |
Reaction Steps
To a stirred solution of 5-[2-benzyloxy-4-(1,2-dibromo-2-phenylethyl)-phenyl]-1,1-dioxo-1,2,5-thiadiazolidin-3-one (25 mg, 0.043 mmol) in MeOH/methylene chloride (1:1, 4 mL) is added NaOMe (0.17 mL, 0.086 mmol, 0.5M in THF). The solution is stirred at RT for 2 h and the solvent is removed under reduced pressure to give the title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084448B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-d69a816039ff44f4a2deb5d516db4bd6 |
| Source note | uspto-grants-2011_12 |