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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 660530Generated: November 1, 2026

Hydrochloric Acid → HCID 24969059, compound

https://huagongshe.com/reaction/660530

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 24969058HCID 24969058—
SolventDiethyl EtherHCID 3283—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 24969059HCID 24969059—

Reaction Steps

To a suspension of 3-[3-hydroxy-4-(1,1,4-trioxo-1,2,5-thiadiazolidin-2-yl)-benzyl]-piperidine-1-carboxylic acid tert-butyl ester (24 mg, 0.052 mmol) in ether (1.5 mL) is added 2 mL of HCl in dioxane (4 M) and the mixture is stirred at RT for 18 h. The solvent is removed under reduced pressure to give the hydrochloride salt of the title compound: (M−1)−=324.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08084448B2
Source datasetuspto-grants-2011_12
ORD IDord-73c626ac225d4422ba1ac779d040c483
Source noteuspto-grants-2011_12