HCID 68839644, compound → HCID 68839806, compound

Participants

Reaction Steps

A solution of 3-{3-benzyloxy-4-[1,1,4-trioxo-5-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-2-yl]-phenyl}-propionic acid tert-butyl ester (420 mg, 0.77 mmol) in 6 mL of TFA/methylene chloride (1:1) is stirred at RT for 20 min. The solvent is removed under reduced pressure. Methylene chloride is added and removed (4×) to give the title compound as an oil: (M−1)−=489.

Provenance & Evidence