Methyl Acrylate → HCID 68920370, compound
Reaction equation
[CH2:1]([O:8][C:9]1[CH:14]=[C:13](I)[CH:12]=[CH:11][C:10]=1[N:16]1[S:20](=[O:22])(=[O:21])[N:19]([CH2:23][CH2:24][Si:25]([CH3:28])([CH3:27])[CH3:26])[C:18](=[O:29])[CH2:17]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:30]([O:34][CH3:35])(=[O:33])[CH:31]=[CH2:32]>>[CH3:35][O:34][C:30](=[O:33])/[CH:31]=[CH:32]/[C:13]1[CH:12]=[CH:11][C:10]([N:16]2[CH2:17][C:18](=[O:29])[N:19]([CH2:23][CH2:24][Si:25]([CH3:28])([CH3:27])[CH3:26])[S:20]2(=[O:22])=[O:21])=[C:9]([O:8][CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH:14]=1Participants
3
Procedure
The title compound is prepared from 5-(2-benzyloxy-4-iodo-phenyl)-1,1-dioxo-2-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-3-one and methyl acrylate analogous to Example 97, step A.
Sources & evidence
- ORD record
- ord-defd296586184be89a2706074586ddcf
- Source dataset
- uspto-grants-2011_12
- Patent number
- US08084448B2
Reaction notes
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