HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 68839036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 15054011 | HCID 15054011 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Acetic acid ethanol | HCID 18476134 | — |
| Product | HCID 68839036 | HCID 68839036 | — |
Reaction Steps
To a solution of 2-benzyloxy-1-nitro-4-trifluoromethylbenzene (1.0 g. 3.4 mmol) in 16 mL HOAc/EtOH (1:3) is added iron powder and the mixture is refluxed for 2 h. The mixture is cooled to RT and water is added and it is extracted with EtOAc. The organic phase is dried over sodium sulfate and the solvent removed under reduced pressure to give the title compound as a reddish oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084448B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-9df361a609464c65961546419f36ac73 |
| Source note | uspto-grants-2011_12 |