N-bromobutanimide → HCID 86632592, compound

Participants

Reaction Conditions

Reaction Steps

To a suspension of NBS (1.60 g, 9.01 mmol) in methylene chloride (20 mL) at 0° C. is added a solution of 2-benzyloxy-3,5-difluorophenylamine (2.12 g, 9.01 mmol) and the mixture is stirred at 0° C. for 30 min then at RT for 30 min. The Mixture is washed with water and the solvent evaporated under reduced pressure. The residue is purified by column chromatography to give the title compound: MS (M−H)−=313.

Provenance & Evidence