HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → Benzophenone imine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | Benzophenone | HCID 3102 | — |
| Solvent | 1,2-Dichlorobenzene | HCID 7239 | — |
| Product | Benzophenone imine | HCID 136809 | 26% |
Reaction Steps
36.2 Grams of benzophenone, 50 ml of o-dichlorobenzene and 0.5 g of benzoic acid were fed to a reactor. Ammonia gas was passed through the reaction mixture under 6 atmospheres at 160° C. of the reaction temperature at a feed rate of 0.2 l/min. (NTP) continuously. The reaction was conducted for 3 hours and benzophenoneimine was obtained in yield of 26%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04130586 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-94d6e3ff66d74ae5a525ed7bb123c0c7 |
| Source note | uspto-grants-1978_12 |