HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68836874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 58012170 | HCID 58012170 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68836874 | HCID 68836874 | — |
Reaction Steps
130 mg (375 μmol) of the compound from Example 174A are stirred at RT in 2 ml of a 4 M solution of hydrogen chloride in dioxan. After complete conversion, the volatile components are removed on the rotary evaporator and the residue dried under high vacuum. 105 mg (99% of theory) of the title compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084481B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-6a5ab579e85447cda0669804a4067e15 |
| Source note | uspto-grants-2011_12 |