huagongshe.com
HRID66095

反应详情

EQUATION

反应方程式

HRID 66095 的结构方程式

REACTANTS

反应物

1
结构：CC1(Oc2ccc([N+](=O)[O-])cc2)C2CC3CC(C2)CC1C3
HCID12510268

未命名化合物

PRODUCTS

生成物

1
结构：CC1(Oc2ccc(N)cc2)C2CC3CC(C2)CC1C3
HCID12510285

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

A solution of 15.0 g. (0.0522 mole) of 4-(2-methyl-2-adamantyloxy)-nitrobenzene in 150 ml. of ethyl acetate was hydrogenated over 10% Pd/C. The crude product was recrystallized from CH2Cl2 and Skellysolve B to give 8.6 g. of light tan solid, m.p. 95.6°-97.9° C.

WORKUP

后处理

  1. customThe crude product was recrystallized from CH2Cl2 and Skellysolve B
  2. customto give 8.6 g