1,4-Dibromobutane → HCID 12510313, compound

HRID 66096Notes

Reaction equation

HRID 66096 reaction equation
[C:1]12([O:11][C:12]3[CH:18]=[CH:17][C:15]([NH2:16])=[CH:14][C:13]=3[Cl:19])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.Br[CH2:21][CH2:22][CH2:23][CH2:24]Br.C(=O)([O-])[O-].[K+].[K+]>C(O)C>[C:1]12([O:11][C:12]3[CH:18]=[CH:17][C:15]([N:16]4[CH2:24][CH2:23][CH2:22][CH2:21]4)=[CH:14][C:13]=3[Cl:19])[CH2:2][CH:3]3[CH2:4][CH:5]([CH2:6][CH:7]([CH2:9]3)[CH2:8]1)[CH2:10]2

Participants

5

Reactant 3

HCID 80561,4-DibromobutaneHCID 11430Potassium CarbonateHCID 12510279HCID 12510279, compound

Product 1

HCID 12510313HCID 12510313, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

1.7 g. (0.00612 Mole) of 4-(1-adamantyloxy)-3-chloroaniline. 1.32 g. (0.00612 mole) of 1,4-dibromobutane and 1.86 g. (0.0135 mole) of potassium carbonate were combined in 50 ml. of absolute ethanol and refluxed for 18 hours.

Sources & evidence

ORD record
ord-8cb3a310d13c40459157fcda578b1dc7
Source dataset
uspto-grants-1978_12
Patent number
US04130561

Reaction notes

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