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HRID661124

反应详情

EQUATION

反应方程式

HRID 661124 的结构方程式

REACTANTS

反应物

2
结构：CCC[CH2][Sn]([CH2]CCC)([CH2]CCC)[c]1cnc(NC(=O)OC(C)(C)C)s1
HCID2763269

tert-Butyl [5-(tributylstannyl)-1,3-thiazol-2-yl]carbamate

C20H38N2O2SSn

结构：Brc1ccc2nnccc2c1
HCID11229560

6-bromocinnoline

C8H5BrN2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)Nc1ncc(-c2ccc3nnccc3c2)s1
HCID86613781

未命名化合物

收率 73.1%

PROCEDURE

实验过程

The title compound (0.24 g, 60%) was synthesized in a manner similar to that described in Example 253 from 6-bromocinnoline (0.25 g, 1.0 mmol) and tert-butyl 5-(tributylstannyl)thiazol-2-ylcarbamate (0.90 g, 1.5 eq). LCMS (API-ES) m/z (%): 329.4 (100%, M++H).