Hydrochloric Acid → HCID 54144080, compound

HRID 66119Notes

Reaction equation

HRID 66119 reaction equation
[OH:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[CH:4]=[CH:5][C:6]1[CH:15]=[CH:14][C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[N:7]=1.[CH3:20][N:21]([CH2:23][CH2:24]Cl)[CH3:22].Cl>>[CH3:20][N:21]([CH3:22])[CH2:23][CH2:24][O:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[CH:4]=[CH:5][C:6]1[CH:15]=[CH:14][C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[N:7]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 79012-Chloro-N,N-dimethylethylamineHCID 28644302-[2-(2-Quinolinyl)ethenyl]phenol

Product 1

HCID 54144080HCID 54144080, compound

Procedure

2-[o-(β-Dimethylamino-ethoxy)-styryl]-quinoline was prepared from 2-(o-hydroxy-styryl)-quinoline (m.p. 274°-278° C.) and dimethylamino-ethyl chloride, and the free base was converted into its monohydrochloride, yielding 86% of theory of the compound of the formula ##STR8## which had a melting point of 188° C.

Workup

  1. customyielding 86% of theory of the compound of the formula ##STR8## which

Sources & evidence

ORD record
ord-138592e6f6b94b03a62624ce5a227f36
Source dataset
uspto-grants-1978_12
Patent number
US04130650

Reaction notes

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