Hydrochloric Acid → HCID 53638845, compound

HRID 66122Notes

Reaction equation

HRID 66122 reaction equation
Cl[CH2:2][CH2:3][O:4][C:5]1[CH:19]=[CH:18][CH:17]=[CH:16][C:6]=1[CH:7]=[CH:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([CH3:15])[N:10]=1.[CH3:20][NH:21][CH3:22].Cl>>[CH3:20][N:21]([CH3:22])[CH2:2][CH2:3][O:4][C:5]1[CH:19]=[CH:18][CH:17]=[CH:16][C:6]=1[CH:7]=[CH:8][C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([CH3:15])[N:10]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 674DimethylamineHCID 543031442-[o-(beta-Chloro-ethoxy)-styryl]-6-methyl-pyridine

Product 1

HCID 53638845HCID 53638845, compound

Procedure

2-[o-(β-Dimethylamino-ethoxy)-styryl]-6-methyl-pyridine was prepared from 2-[o-(β-chloro-ethoxy)-styryl]-6-methyl-pyridine and dimethylamine, and the free base was converted into its monohydrochloride, yielding 45% of theory of the compound of the formula ##STR11## which had a melting point of 200° C.

Workup

  1. customyielding 45% of theory of the compound of the formula ##STR11## which

Sources & evidence

ORD record
ord-b3d7785d4c814887ab7bfb519891f1b9
Source dataset
uspto-grants-1978_12
Patent number
US04130650

Reaction notes

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