HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178524590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178469293 | HCID 178469293 | — |
| Product | HCID 178524590 | HCID 178524590 | — |
Reaction Steps
A mixture of 4,7-dihydro-4,7-dioxo-6-hydroxy-1H-cyclohepta[b]pyridine-2-carboxylic acid ethyl ester (2.5 g, described in Example 3) and 19% hydrochloric acid (75 ml) is refluxed for 1 hour and cooled to room temperature. The crystalline precipitate is collected and washed with water, ethanol and ether to obtain the title compound, mp > 270° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04130649 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-78a56da359094e41b40b68c9b96d18ea |
| Source note | uspto-grants-1978_12 |