HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22755625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4,7-dihydro-4,7-dioxo-2-ethoxycarbonyl-6-[(2-ethoxy-2-oxoethyl)oxy]-1H-cyclohepta[b]pyridine-1-acetic acid ethyl ester | HCID 54323444 | — |
| Product | HCID 22755625 | HCID 22755625 | — |
Reaction Steps
A mixture of 4,7-dihydro-4,7-dioxo-2-ethoxycarbonyl-6-[(2-ethoxy-2-oxoethyl)oxy]-1H-cyclohepta[b]pyridine-1-acetic acid ethyl ester (0.617 g, described in Example 15) and 19% hydrochloric acid (4.2 ml) is refluxed for 1 hr and cooled to room temperature. The precipitate is collected and washed with water, acetone and ether to obtain the title compound, mp > 270° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04130649 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-3e7aff66cd014058a6e40a2d197658b2 |
| Source note | uspto-grants-1978_12 |