1,4-Dioxane hydrochloride → HCID 178479650, compound

Participants

Reaction Conditions

Reaction Steps

4N—HCl/dioxane (100 ml) was added to 4-(2-benzyloxy-pyrimidin-5-yl)-morpholine (8.4 g) and the resulting suspension was stirred at 50° C. for an hour. The reaction mixture was cooled to room temperature and the precipitated solid was collected by filtration, washed with hexane, dried to give the titled compound (7.49 g). MS (m/z): 182 [M+H]+.

Provenance & Evidence