HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Oxobutanoic acid → Isopropylaminium
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Oxobutanoic acid | HCID 1112 | — |
| Reactant | Isopropylamine | HCID 6363 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Isopropylaminium | HCID 3364502 | — |
| Product | 4-Oxobutanoate | HCID 9543238 | — |
Reaction Steps
100 Mg. of 4-(6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyric acid in 15 ml. of hot benzene is treated with 60 mg. of isopropyl amine. The solution is allowed to cool to room temperature and the product is filtered off, washed with ether and dried to yield isopropylammonium 4-(6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04130654 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-9fbbeabf522d4d0bb714410dabecfb77 |
| Source note | uspto-grants-1978_12 |