HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumarate → 3',4'-Dichloro-2-(2-pyrrolidinylidene)-acetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumarate | HCID 5460307 | — |
| Reactant | 2-[2-(3,4-Dichlorophenyl)-2-(cyclohexylimino)-ethylidene]-pyrrolidine- | HCID 137195921 | — |
| Solvent | Diethyl ether 2-propanol | HCID 22147583 | — |
| Product | 3',4'-Dichloro-2-(2-pyrrolidinylidene)-acetophenone | HCID 70573167 | — |
Reaction Steps
With the use of 76.8 g (0.3 mole) of 3',4'-dichloro-2-(2-pyrrolidinylidene)-acetophenone, there is obtained in an analogous manner 2-[2-(3,4-dichlorophenyl)-2-(cyclohexylimino)-ethylidene]-pyrrolidine-(1:1)-fumarate, m.p. 208°-209° (from isopropanol/ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04130652 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-5c5d6aca6ead40eb8ac759af48ed87ac |
| Source note | uspto-grants-1978_12 |