HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → Hexahydro-2a1H-2a,4a,6a-triazacyclopenta[cd]pentalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 1,4,7-Triazacyclononane | HCID 188318 | — |
| Product | Hexahydro-2a1H-2a,4a,6a-triazacyclopenta[cd]pentalene | HCID 10986308 | — |
Reaction Steps
In a manner similar to that of Example 1 (C), 4.55 g (35.5 mmol) of 1,4,7-triazacyclononane and 4.20 g of dimethylformamide dimethyl acetal were reacted to give 4.33 g (88%) clear, colorless liquid, bp 79°-80° (2.6mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04130715 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-64791c2b857b46bbad90fb33b83063ec |
| Source note | uspto-grants-1978_12 |