HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178479594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178514627 | HCID 178514627 | — |
| Product | HCID 178479594 | HCID 178479594 | — |
Reaction Steps
A suspension of 3 g of N2 -(2-phenoxathiinylsulfonyl)-L-arginine in 20 ml of thionyl chloride was stirred for 2 hours at room temperature. Addition of cold dry diethyl ether resulted in a precipitate which was collected by filtration and washed several times with dry diethyl ether to give N2 -(2-phenoxathiinylsulfonyl)-L-arginyl chloride hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04131673 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-230cf04c0f214fd6b4278fd6736d9fdd |
| Source note | uspto-grants-1978_12 |