Water → 2-Chloro-1-(2-methoxyphenyl)ethan-1-ol

Beteiligte Stoffe

Reaktionsschritte

1.7 g of 2-methoxy-α-chloroacetophenone are dissolved in 30 ml of dioxane, and 12 ml of water are added thereto. 600 mg of sodium borohydride are added gradually to the solution at 10° to 20° C. Then, the mixture is treated in the same manner as described in Example 2-(1). 1.4 g of α-chloromethyl-2-methoxybenzylalcohol are obtained as a crude oil.

Herkunft & Nachweise