HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzoyl chloride → 5-Benzoylamino-2-phenyloxazolo[5,4-b]pyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzoyl chloride | HCID 7412 | — |
| Edukt | 5-Amino-2-phenyloxazolo[5,4-b]pyridine | HCID 22754793 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | 5-Benzoylamino-2-phenyloxazolo[5,4-b]pyridine | HCID 22754798 | — |
Reaktionsschritte
A solution of 80 mg. of 5-amino-2-phenyloxazolo[5,4-b]pyridine in 1 ml. of pyridine was treated with 0.07 ml. of benzoyl chloride. After standing 1 hour the mixture was diluted with ice-water. The precipitate was collected and recrystallized from methanol to give 5-benzoylamino-2-phenyloxazolo[5,4-b]pyridine, m.p. 191°-192° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04131677 |
| Quelldatensatz | uspto-grants-1978_12 |
| ORD ID | ord-3eade76e1ede47acad219115495f1cd5 |
| Quellennotiz | uspto-grants-1978_12 |